Title: Liquid Chromatographic Determination of Deoxynivalenol in Baby Food and Animal Feed: Interlaboratory Study.
Authors: STROKA JOERGDERBYSHIRE MichelleMISCHKE CARSTENAMBROSIO MASSIMOKROEGER KATYARRANZ HERNANDEZ ISABEL
Citation: JOURNAL OF AOAC INTERNATIONAL vol. 89 no. 4 p. 1012-1020
Publisher: AOAC INTERNATIONAL
Publication Year: 2006
JRC N°: JRC34480
URI: http://publications.jrc.ec.europa.eu/repository/handle/JRC34480
Type: Articles in Journals
Abstract: An interlaboratory study was conducted for the determination of deoxynivalenol in baby food and animal feed by high-performance liquid chromatography with UV detection. The study included 4 participants representing a cross section of industry, official food control, and research facilities. Mean recoveries reported ranged from 89% (at 120μg/kg) to 85% (at 240μg/kg) for baby food and from 100% (at 200μg/kg) to 93% (at 400μg/kg) for animal feed. On the basis of the results for spiked samples (blind duplicates at 2 levels), as well as those for naturally contaminated samples (blind duplicates at 3 levels), the relative standard deviation for repeatability (RSDr) in analyses of baby food ranged from 6.4 to 14% and in analyses of animal feed, from 6.1 to 16.5%.
JRC Institute:Institute for Reference Materials and Measurements

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