Title: Preparation and Certification of the Isotopic Reference Material IRMM-049d
Authors: JAKOPIC RozleEYKENS RogerKEHOE FrancesKUEHN HeinzRICHTER StephanVERBRUGGEN AndreAREGBE Yetunde
Publisher: Publications Office of the European Union
Publication Year: 2011
JRC Publication N°: JRC66016
ISBN: 978-92-79-20992-5 (print), 978-92-79-20993-2 (pdf)
ISSN: 1018-5593 (print), 1831-9424 (pdf)
Other Identifiers: EUR 24915 EN
OPOCE LA-NA-24915-EN-C (print), LA-NA-24915-EN-N (pdf)
URI: http://publications.jrc.ec.europa.eu/repository/handle/JRC66016
DOI: 10.2787/49209 (print)
10.2787/49418 (pdf)
Type: EUR - Scientific and Technical Research Reports
Abstract: A highly enriched 242Pu Isotopic Reference Material (IRMM-049d) has been prepared and certified for the 242Pu isotope amount content. The certified value of 3.666 8(18) x 10-7 mol 242Pu per g of solution was established by Isotope Dilution Mass Spectrometry (IDMS). The plutonium isotopic composition was determined by Thermal Ionization Mass Spectrometry (TIMS) and calibration of these measurements by means of synthetic mixtures. The IRMM-049d Isotopic Reference Material is supplied in a glass ampoule with a screw cap seals containing about 10 mL of 5 mol x L-1 nitric acid with plutonium. The content of each vial is approximately 1 mg 242Pu. This Isotopic Reference Material is the product of a systematic IRMM programme to supply Isotopic Reference Materials of various isotopes at different concentrations.
JRC Institute:Institute for Reference Materials and Measurements

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