Title: Collaborative investigation of matrix effects in mycotoxin determination by high performance liquid chromatography coupled to mass spectometry
Authors: MALACHOVA AlexandraSULYOK MichaelSCHUHMACHER M.BERTHILLER FranzHAJSLOVA JanaVEPRIKOVA ZdenkaZACHARIASOVA MilenaLATTANZIO VeronicaDE SAEGER SarahDI MAVUNGU JoseMALYSHEVA SvetlanaBISELLI SWINKELMANN OleBREIDBACH AndreasHERD SimonKRSKA Rudolf
Citation: QUALITY ASSURANCE AND SAFETY OF CROPS & FOODS vol. 5 no. number 2 p. 91-103
Publisher: WILEY-BLACKWELL
Publication Year: 2013
JRC N°: JRC80160
ISSN: 1757-8361
URI: http://publications.jrc.ec.europa.eu/repository/handle/JRC80160
DOI: 10.3920/QAS2012.0213
Type: Articles in periodicals and books
Abstract: Introduction LC-MS is a commonly used technique for mycotoxin determination in food and feed. However, accuracy and reliability of the obtained results can suffer from ion suppression/enhancement caused by co-eluting matrix components. Objective Inter-Laboratory study concerning relative and absolute matrix effects (MEs) in various food and feed matrices was carried out. The applicability of commonly used strategies in ME reduction were tested in quantitative determination of nivalenol, deoxynivalenol, and fumonisn B1 and B2.
JRC Directorate:Health, Consumers and Reference Materials

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