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Certification of the mass fraction of 3- and 2-MCPD fatty acid esters in infant formula: ERM®-BD087

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ERM-BD087 is an infant formula reference material certified for the mass fraction of the fatty acid esters of 3-chloro-1,2-propanediol (3-MCPD) and the sum of 3-MCPD and 3-MCPD fatty acid esters, the fatty acid esters of 2-MCPD and the sum of 2-MCPD and 2-MCPD fatty acid esters. The material was produced, using a contaminated coconut oil in the recipe. Between-unit homogeneity was quantified and stability during transport and storage was assessed in accordance with ISO Guide 35:2017. The material was characterised by an inter-laboratory comparison of laboratories of demonstrated competence and adhering to ISO/IEC 17025:2017. Technically invalid results were removed but no outlier was eliminated since no technical reason for deviations was found. Uncertainties of the certified values were calculated in accordance with ISO 17034:2016 and ISO Guide 35:2017 and include uncertainties related to possible inhomogeneity, instability and characterisation. The material is intended for the quality control and assessment of method performance.
2023-12-05
Publications Office of the European Union
JRC135734
978-92-68-09499-0 (online),   
OP KJ-09-23-546-EN-N (online),   
https://publications.jrc.ec.europa.eu/repository/handle/JRC135734,   
10.2760/63251 (online),   
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