Two reference materials with certified mass fractions of SY124 in gas oil have been prepared. Samples were prepared by spiking of blank gas oil with pure SY124. Homogeneity and stability were confirmed and maximum heterogeneity and degradation were estimated. Purity of the SY124 used for spiking was determined using thermogravimetric analysis, high-performance liquid chromatography with UV detection, gas chromatography with flame ionisation and mass spectrometric detection, nuclear magnetic resonance and Karl Fischer titration. Full uncertainty budgets comprising all potential uncertainty sources were established. The following mass fractions were derived: ERM-EF317: 0.141 +- 0.018 mg.kg-1; ERM-EF318: 7.0 +- 0.04 mg.kg-1.
LINSINGER Thomas;
KOOMEN Ger;
EMTEBORG Hakan;
ROEBBEN Gert;
KRAMER Gerard;
LAMBERTY Andree;
2006-03-31
AMER CHEMICAL SOC
JRC30360
https://publications.jrc.ec.europa.eu/repository/handle/JRC30360,
10.1021/ef0501492,
| Name | Country | City | Type |
|---|
This document is only visible at the Commission level.
You are not authorized to publish or distribute it outside the European Commission.
This is a public document. You can share this publication.
Datasets
| ID | Title | Public URL |
|---|
Dataset collections
| ID | Acronym | Title | Public URL |
|---|
Scripts / source codes
| Description | Public URL |
|---|
Additional supporting files
| File name | Description | File type |
|---|