Please use this identifier to cite or link to this item:
|Title:||Production of Two Certified Reference Materials for the Determination of SY 124 (Euromarker) in Gas Oil|
|Authors:||LINSINGER THOMAS; KOOMEN Ger; EMTEBORG HAKAN; ROEBBEN GERT; KRAMER Gerard; LAMBERTY ANDREE|
|Citation:||ENERGY & FUELS vol. 19 p. 2460-2465|
|Publisher:||AMER CHEMICAL SOC|
|Type:||Articles in periodicals and books|
|Abstract:||Two reference materials with certified mass fractions of SY124 in gas oil have been prepared. Samples were prepared by spiking of blank gas oil with pure SY124. Homogeneity and stability were confirmed and maximum heterogeneity and degradation were estimated. Purity of the SY124 used for spiking was determined using thermogravimetric analysis, high-performance liquid chromatography with UV detection, gas chromatography with flame ionisation and mass spectrometric detection, nuclear magnetic resonance and Karl Fischer titration. Full uncertainty budgets comprising all potential uncertainty sources were established. The following mass fractions were derived: ERM-EF317: 0.141 +- 0.018 mg.kg-1; ERM-EF318: 7.0 +- 0.04 mg.kg-1.|
|JRC Directorate:||Health, Consumers and Reference Materials|
Files in This Item:
There are no files associated with this item.
Items in repository are protected by copyright, with all rights reserved, unless otherwise indicated.