A new LC-MS/MS method has been developed for the multiresidue determination of 11 (fluoro)quinolone antibiotics (FQs), including acidic and aphoteric speices, around their maximum residue level (MRL) in pig kidney. The procedure involved a common sample preparation by solid-phase extraction on disposable extraction cartridges followed by a fast reversed-phase liquid chromatography-tandem mass spectrometry analysis. The method was validated according to the Commission Decision 2002/657/CE. The accuracy of the method was satisfactory with recoveries included in the interval 80-100%. The precision results showed mean repeatability and reproducibility coefficients of 7.4% and 11.8% respectively. Limits of quantification much lower than the MRLs could be obtained.
TOUSSAINT Brigitte;
CHEDIN Mostafa;
BORDIN Guy;
RODRIGUEZ Adela;
2006-03-28
ELSEVIER
JRC32898
https://publications.jrc.ec.europa.eu/repository/handle/JRC32898,
| Name | Country | City | Type |
|---|
This document is only visible at the Commission level.
You are not authorized to publish or distribute it outside the European Commission.
This is a public document. You can share this publication.
Datasets
| ID | Title | Public URL |
|---|
Dataset collections
| ID | Acronym | Title | Public URL |
|---|
Scripts / source codes
| Description | Public URL |
|---|
Additional supporting files
| File name | Description | File type |
|---|