Please use this identifier to cite or link to this item:
|Title:||Determination of (fluoro)Quinolone Antibiotic Residues in Pig Kidney Using Liquid Chromatography-tandem Mass Spectrometry Part II: Intercomparison Exercise|
|Authors:||TOUSSAINT BRIGITTE; CHEDIN MOSTAFA; VINCENT URSULA; BORDIN GUY|
|Citation:||JOURNAL OF CHROMATOGRAPHY A vol. 1088 p. 40-48|
|Publisher:||ELSEVIER SCIENCE BV|
|Type:||Articles in periodicals and books|
|Abstract:||A recently in-house validated method for the liquid chromatography-tandem mass spectrometry (LC-MS/MS) determination of eleven (fluoro)quinolone antibiotics (FQs) in pig kidney has been fully validated through an intercomparison exercise. This ring trial involved eight European Laboratories and was based on the Commission Decision 2002/657/CE for validation of method and on the IUPAC protocol for method performances studies. The laboratories data were submitted to a one-way analysis of variance. Satisfactory results were obtained for each FQ with regards to within- and between-laboratory reproducibility and accuracy. The method was validated for the simultaneous qualitative and quantitative determination of the eleven FQs in pig kidney around their maximum residue limit (MRL) as defined in the European Council Regulation 2377/90/EEC.|
|JRC Directorate:||Health, Consumers and Reference Materials|
Files in This Item:
There are no files associated with this item.
Items in repository are protected by copyright, with all rights reserved, unless otherwise indicated.