Collaborative investigation of matrix effects in mycotoxin determination by high performance liquid chromatography coupled to mass spectometry
Introduction LC-MS is a commonly used technique for mycotoxin determination in food and feed. However, accuracy and reliability of the obtained results can suffer from ion suppression/enhancement caused by co-eluting matrix components. Objective Inter-Laboratory study concerning relative and absolute matrix effects (MEs) in various food and feed matrices was carried out. The applicability of commonly used strategies in ME reduction were tested in quantitative determination of nivalenol, deoxynivalenol, and fumonisn B1 and B2.
MALACHOVA Alexandra;
SULYOK Michael;
SCHUHMACHER M.;
BERTHILLER Franz;
HAJSLOVA Jana;
VEPRIKOVA Zdenka;
ZACHARIASOVA Milena;
LATTANZIO Veronica;
DE SAEGER Sarah;
DI MAVUNGU Jose;
MALYSHEVA Svetlana;
BISELLI S;
WINKELMANN Ole;
BREIDBACH Andreas;
HERD Simon;
KRSKA Rudolf;
2017-03-17
WILEY-BLACKWELL
JRC80160
1757-8361,
https://publications.jrc.ec.europa.eu/repository/handle/JRC80160,
10.3920/QAS2012.0213,
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