Comparison of XRD, XANES and TGA methods to assess the O/M ratio of Th0.60Am0.40O2-x

PRIEUR, Damien; VIGIER, Jean-Francois; ROTHE, J.; SOMERS, Joseph

doi:10.1016/j.jnucmat.2014.01.031

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Comparison of XRD, XANES and TGA methods to assess the O/M ratio of Th0.60Am0.40O2-x

The mixed oxide Th0.60Am0.40O2-x has been synthesized and characterized after reductive and oxidative thermal treatments. Both materials are monophasic solid solutions. The determination of O/M ratio was achieved combining XRD, XANES and TGA, showing the consistence between the three methods. This study represents a further step in our investigation of the Th-Am-O system and improves it comprehension.

PRIEUR Damien; VIGIER Jean-Francois; ROTHE J.; SOMERS Joseph;

2014-03-07

ELSEVIER SCIENCE BV

JRC86874

0022-3115,

http://www.sciencedirect.com/science/article/pii/S0022311514000427, https://publications.jrc.ec.europa.eu/repository/handle/JRC86874,

10.1016/j.jnucmat.2014.01.031,

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